Measured Data

Specific Heat

Experiments for specific heat [J/(kg K)], or heat capacity, were conducted using a heat flow meter on unconditioned and dried samples at 10 °C, 20 °C, 30 °C and 40 °C.

Unconditioned

Temperature (C) Specific Heat Mean (J/kg-K) Standard Deviation (J/kg-K)
10.0 1533.0 366.0
20.0 1598.0 388.0
30.0 1674.0 403.0
40.0 1741.0 417.0

Thermal Conductivity

Experiments for thermal conductivity [k] were conducted using a heat flow meter on unconditioned samples at 15 °C and 45 °C.

Unconditioned

Temperature (C) Conductivity Mean (W/m-K) Standard Deviation (W/m-K)
15.0 0.045 0.001
45.0 0.050 0.001

Mass Loss Rate (MLR)

Initial-mass-normalized mass loss rate [1/s] was measured in the simultaneous thermal analyzer experiments at three heating rates: 3 K/min, 10 K/min, and 30 K/min and mass loss rate [g/s] in the cone calorimeter at three heat fluxes: 25 kW/m2, 50 kW/m2, and 75 kW/m2.

Cone Calorimeter Test Notes:
Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.

Simultaneous Thermal Analyzer

Cone Calorimeter: 25 kW/m2

Cone Calorimeter: 50 kW/m2

Cone Calorimeter: 75 kW/m2

Heat Release Rate Per Unit Area (HRRPUA)

Experiments for heat release per unit area [kW/m2] were conducted on samples conditioned at 20°C and 50% relative humidity using a cone calorimeter at three different heat fluxes: 25 kW/m2, 50 kW/m2, and 75 kW/m2.

Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.

Cone Calorimeter: 25 kW/m2

Cone Calorimeter: 50 kW/m2

Cone Calorimeter: 75 kW/m2

Carbon Monoxide (CO) Yield

Carbon monoxide yield was measured during cone calorimeter experiments conducted at heat fluxes of 25 kW/m2, 50 kW/m2, and 75 kW/m2.

Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.

Incident Heat Flux [kW/m²] Mean CO Yield [g/g] CO Yield Std. Dev. [g/g]
25 0.047 0.027
50 0.026 0.002
75 0.009 0.002

Specific Heat Release Rate

Experiments for specific heat release rate [W/g], were conducted using a micro-scale combustion calorimeter at a heating rate of 30 K/min.

Derived Data

Effective Heat of Combustion (Δhc)

Effective heat of combustion [MJ/kg] is calculated from data collected in both micro-scale combustion calorimeter experiments and cone calorimeter experiments.

Cone Calorimeter Test Notes:
Samples were tested without compression of the material. The sample preparation consisted of filling a pre-formed, 5 cm deep aluminum foil tray with cellulose insulation, and attempting to achieve homogenous packing density. At the 50 kW/m2 and 75 kW/m2 exposures, ignition occurred in less than 1 second -- faster than the recorded time.

Micro-scale Combustion Calorimeter

Value R1 R2 R3 Mean Std. Dev.
Heat of Combustion (MJ/kg) 6.7 5.79 6.29 6.26 0.37

Cone Calorimeter

Incident Heat Flux [kW/m²] Mean Effective Heat of Combustion [MJ/kg] Effective Heat of Combustion Std. Dev. [MJ/kg]
25 10.3 0.2
50 12.1 0.4
75 12.4 0.6

Band Averaged Emissivity

Band averaged emissivity was calculated from reflectance measurements conducted with an integrating sphere and Fourier transform infrared spectrometer.

Source Temperature [K] Emissivity Std. Dev.
600.0 0.889 0.002
800.0 0.855 0.003
1000.0 0.819 0.005
1200.0 0.783 0.007
1400.0 0.751 0.010
1600.0 0.724 0.012
1800.0 0.702 0.015
2000.0 0.685 0.017